Plane-strain bulge test for nanocrystalline copper thin films

Xiaoding WEI*, Dongyun LEE, Sanghoon SHIM, Xi CHEN, Jeffrey W. KYSAR

*Corresponding author for this work

Research output: Journal PublicationsJournal Article (refereed)peer-review

33 Citations (Scopus)

Abstract

Free-standing nanocrystalline Cu films with grain size around 39 nm are fabricated by thermal evaporation and characterized by the plane-strain bulge test. Young's modulus and yield stress at a 0.2% offset are about 110-130 GPa and 400 MPa, respectively. Results show that the strength of the n-Cu films is largely independent of film thickness at a strain rate less than 10-5s-1. No grain growth is observed and the predominant plastic deformation mechanism is grain boundary sliding accompanied by dislocation mechanisms. © 2007 Acta Materialia Inc.
Original languageEnglish
Pages (from-to)541-544
Number of pages4
JournalScripta Materialia
Volume57
Issue number6
DOIs
Publication statusPublished - 2007
Externally publishedYes

Bibliographical note

Supports from NSF DMR-0650555, NSF CMMI-0500239, from the Academic Quality Fund of Columbia University, and NSF CMS-0407743, are gratefully acknowledged. In addition, this work was supported in part by the MRSEC Program of the National Science Foundation under Award Number DMR-0213574 and by the New York State Office of Science, Technology and Academic Research (NYSTAR). The authors also thank Prof. J. Vlassak and his research group for very helpful discussions.

Keywords

  • Bulge test
  • Nanocrystalline materials
  • Thin films

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